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  • 1. Hansbo, Anita
    et al.
    Nylén, Per
    Models for the simulation of spray deposition and robot motion optimization in thermal spraying of rotating objects1999Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 122, nr 2-3, s. 191-201Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    In this paper we consider methods to simulate deposit build-up in thermal spraying and to optimize the robot motion so as to obtain the desired layer thickness. We derive a simplified mathematical model for spray deposition on a rotating large object with a smooth, rotationally symmetric, curved surface, yet allowing varying spray distance and direction. Further, we discuss how to obtain and incorporate an empirically determined deposit rate model. In particular, the simplified spray deposition model is chosen to make possible a reasonably cheap method to approximate a deposit rate from the results of layer thickness measurements. We also propose an iterative method to obtain good initial values for robot feed optimization. Numerical examples are presented. © 1999 Elsevier Science S.A.

  • 2.
    Iqbal, Muhammad Ahsan
    et al.
    Department of Industrial Engineering, University of Trento, TN, Italy.
    Secchi, Maria
    Department of Industrial Engineering, University of Trento, TN, Italy.
    Iqbal, Muhammad Adeel
    Department of Mechanical and Aerospace Engineering, Air University Islamabad, Pakistan.
    Montagna, Maurizio
    Department of Physics, University of Trento, TN, Italy.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Fedel, Michele
    Department of Industrial Engineering, University of Trento, TN, Italy.
    MgAl-LDH/graphene protective film: Insight into LDH-graphene interaction2020Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 401, artikel-id 126253Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    MgAl-layered double hydroxides (LDHs) thin films, exhibiting two distinct surface morphologies (Platelet and Cauliflower-like), were synthesized directly on the aluminum substrate. The as-prepared films were further modified with graphene due to the chemical inertness of graphene and its capability to act as a possible physical barrier against ionic media. The morphology and structure of MgAl-LDH/graphene composite films are fully characterized. The corrosion resistance properties were analyzed through Electrochemical impedance spectroscopy and the results were further fitted using “ZSimpWin” software to evaluate coating behavior. The graphene was found to interact with the LDH structure and provide another pathway for the corrosion reactions and results in improve LDHs corrosion resistance properties. The sealing effect of graphene resists the aggressive media penetration and caused an increase of one order magnitude in impedance modulus of MgAl-LDHs. The enhancement in corrosion resistance properties is attributed to the graphene impermeable behavior against corrosive species confirmed by physical and electrochemical characterizations.

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  • 3. Papachristos, V.
    et al.
    Panagoupolos, C.
    Leisner, Peter
    Högskolan i Jönköping, Tekniska Högskolan, JTH, Data- och elektroteknik.
    Olsen, M.
    Wahlstrom, U.
    Sliding Wear Behaviour of Ni-P-W Composition Modulated Coatings1998Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 105, nr 3, s. 224-231Artikel i tidskrift (Refereegranskat)
  • 4.
    Pinate, Santiago
    et al.
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Ispas, A.
    Technische Universität Ilmenau, Ilmenau, Germany.
    Leisner, Peter
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Electrocodeposition of Ni composites and surface treatment of SiC nano-particles2021Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 406, artikel-id 126663Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    This work has explored the surface modification of SiC submicron- and nanoparticles, and its influence on the particles' chemical behaviour and deposition rate in the electroplating of composite Ni/SiC coatings. SiC particles with different sizes (50, 60, 300 and 500 nm) were codeposited in their “as-produced” state. The ζ-potential measurements and alkaline titration for the “as-produced” particles showed differences in chemical behaviour for particles of different sizes, reporting pH buffering effect, even though the particles were inert and chemically the same (SiC). A surface treatment (ST) based on nitric acid was developed in an attempt to set a similar surface state, therefore a similar chemical behaviour in all particles. The ζ-potential measurements and alkaline titration of the “surface treated” particles showed similar results, independently of the size of particles. The pH buffering effect also decreased considerably by the ST. The codeposition rate was modified by the ST differently for each size compared to their as-produced state. The content of SiC50 and SiC500 was doubled (≈2% and ≈19%), tripled for SiC300 (≈7%) and more than halved for SiC60 (≈2%). The microhardness of these composite deposits was linked to the changes in the SiC codeposition.

  • 5.
    Pinate, Santiago
    et al.
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Leisner, Peter
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Wear resistance and self-lubrication of electrodeposited Ni-SiC:MoS2 mixed particles composite coatings2021Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 421, artikel-id 127400Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    Ni-based mixed particles composite coatings were designed to achieve superior wear resistance by combining hard carbides and solid lubricants as a reinforcing particles mix. Pure nickel and single-particles composites were electrodeposited in the same conditions for benchmarking. A pre-study was carried out to optimise the current density to avoid loss of process efficiency due to hydrogen evolution. The production process was also improved by employing ultrasounds to avoid porosity and dendritic growth in the metal caused by conductive MoS2 particles. The presence of MoS2 particles led to nanocrystallinity in the nickel matrix, confirmed by electron backscatter diffraction (EBSD) maps and transmission electron microscopy (TEM). The microstructural changes and codeposition in the different composites were correlated to microhardness and pin-on-disc tests. An extremely high hardness was observed in the mixed particles composite (≈1110 HV) due to the combined effect of the nanocrystalline matrix and high codeposition rate (≈15 vol% SiC and ≈8 vol% MoS2). The codeposition of MoS2 particles provided a self-lubrication capability to the coating, reducing the friction coefficient compared to pure Ni from 0.15 to 0.07. The wear rate was reduced more than 12 times by the mixed reinforcement compared to pure Ni and more than 6 times compared to Ni-SiC.

  • 6.
    Sainis, Salil
    et al.
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Roșoiu, Sabrina
    Centre for Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Ghassemali, Ehsan
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    The role of microstructure and cathodic intermetallics in localised deposition mechanism of conversion compounds on Al (Si, Fe, Cu) alloy2020Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 402, artikel-id 126502Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    Cerium-based conversion coating formation is triggered by a local rise in pH at cathodic sites produced by the oxygen reduction reaction. Therefore, size, morphology distribution and electrochemical potential of those sites play a crucial role. While the deposition reaction is sensitive to both immersion bath concentrations and underlying substrate microstructure, only the former has been widely investigated. This research attempts to fill the gap by studying the effect of controlled microstructure variables like the cathodic intermetallics' geometry and spatial distribution on the conversion compound deposit initiation. A controlled cast Al alloy was synthesised for this study and consisted of distinct cathodic phases: Cu-rich intermetallics, Fe-rich intermetallics and Si particles. The localised deposition preferentially formed only on strong cathodic Cu-rich intermetallics. Size (surface area) of the Cu-rich intermetallic correlated linearly with the deposited area over it in terms of lateral and z-direction spread. The pH gradient occurring from the oxygen reduction near an IM is very local and does not affect pH gradients of a neighbouring IM. When immersion time is increased from 0.5 h to 1 h, the percentage of Cu-rich IM covered with conversion coating increases. Big Cu-rich IM activate faster for deposition reaction than small Cu-rich IM.

  • 7.
    Sarius, N.G.
    et al.
    Högskolan i Jönköping, Tekniska Högskolan, JTH. Forskningsmiljö Material och tillverkning - Ytteknik.
    Lauridsen, J.
    Thin Film Physics Division, Department of Physics, IFM, Linköping University, Linköping, Sweden.
    Lewin, E.
    Department of Materials Chemistry, The Ångström Laboratory, Uppsala University, Uppsala, Sweden.
    Lu, J.
    Thin Film Physics Division, Department of Physics, IFM, Linköping University, Linköping, Sweden.
    Högberg, H.
    Thin Film Physics Division, Department of Physics, IFM, Linköping University, Linköping, Sweden.
    Öberg, Å.
    ABB Corporate Research, Västerås, Sweden.
    Ljungcrantz, H.
    Impact Coatings AB, Linköping, Sweden.
    Leisner, Peter
    Högskolan i Jönköping, Tekniska Högskolan, JTH. Forskningsmiljö Material och tillverkning - Ytteknik.
    Eklund, P.
    Thin Film Physics Division, Department of Physics, IFM, Linköping University, Linköping, Sweden.
    Hultman, L.
    Thin Film Physics Division, Department of Physics, IFM, Linköping University, Linköping, Sweden.
    Ni and Ti diffusion barrier layers between Ti-Si-C and Ti-Si-C-Ag nanocomposite coatings and Cu-based substrates2012Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 206, nr 8-9, s. 2558-2565Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    Sputtered Ni and Ti layers were investigated as a diffusion barrier to substitute electroplated Ni between Ti–Si–C and Ti–Si–C–Ag nanocomposite coatings and Cu or CuSn substrates. Samples were subjected to thermal annealing studies by exposure to 400 °C for 11 h. Dense diffusion barrier and coating hindered Cu from diffusing to the surface. This condition was achieved for electroplated Ni in combination with magnetron-sputtered Ti–Si–C and Ti–Si–C–Ag layers deposited at 230 °C and 300 °C, and sputtered Ti or Ni layers in combination with Ti–Si–C–Ag deposited at 300 °C.

  • 8.
    Sieber, Maximilian
    et al.
    Chemnitz University of Technology, Institute of Materials Science and Engineering, Chemnitz, Germany.
    Mehner, T.
    Dietrich, D.
    Alisch, G.
    Nickel, D.
    Meyer, D.
    Scharf, I.
    Lampke, T.
    Wear-resistant coatings on aluminium produced by plasma anodising - A correlation of wear properties, microstructure, phase composition and distribution2014Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 240, s. 96-102Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    In the recent decades, various process windows have been found for plasma anodising of aluminium surfaces to produce wear-resistant alumina coatings. The coatings offer a high hardness and provide an excellent bonding to the substrate material, thus preventing spallation under mechanical or tribological load. In the present study, coatings with a high abrasive wear resistance and a hardness of up to 12GPa were produced in an electrolyte of 5g/l sodium metasilicate and 5g/l potassium hydroxide at a current density of 30A/dm2. To understand the reasons for the high wear resistance, the morphology as well as the phase composition and distribution within the coating were examined globally and locally using X-ray diffraction with conventional and grazing incidence and electron backscatter diffraction. The analyses show that the coating globally is comprised of approximately one third of α-alumina, one third of γ-alumina and one third of amorphous alumina with locally varying phase content. 

  • 9.
    Sieber, Maximilian
    et al.
    Chemnitz University of Technology, Materials and Surface Engineering Group, Chemnitz, Germany.
    Morgenstern, R.
    Lampke, T.
    Anodic oxidation of the AlCu4Mg1 aluminium alloy with dynamic current control2016Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 302, s. 515-522Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    The anodic oxidation process is a common method for the surface modification of aluminium and its alloys. The increasing application of high-strength aluminium alloys therefore represents a challenge, since alloying elements, amongst them copper, significantly disturb the coating formation during anodising. Hence, flaws arise in the oxide layers and lead to the deterioration of their performance. Recent investigations have indicated the possibility of extenuating the negative influence of the alloying elements on the coating formation by applying time-variable electrical regimes. In case of the current density as the control factor in the coating process, this approach is related to as dynamic current control. For the anodic oxidation of AlCu4Mg1 (EN AW-2024), the effect of dynamic current control on the oxide layer properties is investigated by using a design of experiments (DOE). The parameter variation includes starting ramps, a step-wise change of the current density in the process and pulse current at electrolyte temperatures of 5 °C and 15 °C. A solution of 20 vol% sulphuric acid with an addition of oxalic acid or nitric acid is used as the electrolyte. The produced oxide coatings are examined with regard to their thickness, hardness, their performance in the scratch test and their current density-potential behaviour in diluted NaCl solution. Further, the electrical energy consumption during the anodisation is considered. The results are evaluated with the help of an analysis of variance (ANOVA).

  • 10. Simchen, F.
    et al.
    Sieber, Maximilian
    Materials and Surface Engineering Group, Chemnitz University of Technology, Institute of Materials Science and Engineering, Chemnitz, Germany.
    Lampke, T.
    Electrolyte influence on ignition of plasma electrolytic oxidation processes on light metals2017Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 315, s. 205-213Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    Plasma electrolytic oxidation (PEO), also called plasma anodizing or micro arc oxidation (MAO), is an appropriate method to improve surface characteristics of valve metals. Micro arc discharges, which appear at the working piece in an aqueous electrolyte under strong anodic polarization, are typical for this process. The discharge initiation is discussed controversially. Contradicting theories, which are mainly based on investigations of tantalum, exist concerning the meaning of electrolytic anions, which are initially incorporated in the anodic film. Dual step polarization and PEO experiments were carried out on aluminum, magnesium, and titanium, which are in practical use as lightweight construction materials. For Al 99.5, AZ31, and TiAl6V4 it could be shown that the incorporation of electrolytic anions in the anodic film is not required for the ignition process. Also, the influence of electrolyte conductivity on the ignition voltage was investigated by polarization experiments with silicate, aluminate, and hydroxide solutions using the example of AZ31. It has been demonstrated that not the electrical electrolyte conductivity, but its specific electron injection ability at the electrolyte/substrate interface defines the ignition voltage. This injection ability depends on the kind and concentration of the electrolytic anions.

  • 11.
    State, S. P.
    et al.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Costovici, S.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Mousavi, M.
    Department of Materials Science and Engineering, Delft University of Technology, Mekelweg 2, Delft, 2628 CD, Netherlands.
    Garcia, Y. G.
    Department of Materials Science and Engineering, Delft University of Technology, Mekelweg 2, Delft, 2628 CD, Netherlands.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Cojocaru, A.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Anicai, L.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Visan, T.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Enachescu, M.
    Center of Surface Science and Nanotechnology, University Politehnica of Bucharest, Splaiul Independentei 313, Bucharest, 060042, Romania.
    Electrodeposited Sn-Cu-Ni alloys as lead-free solders on copper substrate using deep eutectic solvents: The influence of electrodeposition mode on the morphology, composition and corrosion behaviour2024Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 477, artikel-id 130324Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    In this work we present the pulsed current (PC) electrodeposition of Sn-Cu-Ni alloy as lead-free solder candidate, from choline chloride – ethylene glycol eutectic mixtures (1:2 molar ratio) onto copper metallic substrates. Electrolytes containing Sn2+, Cu2+ and Ni2+ salts in the selected deep eutectic solvent have been considered. The effect of the applied frequency of PC on the morphology, composition and melting point of the alloy is discussed and compared to the ones obtained using direct current (DC) plating mode. A refinement of the grain size and lower melting temperature of the alloy were noticed when pulsed current was applied. A comparative analysis of the electrochemical corrosion behaviour at macro- and micro- scale has been performed in 0.5 M and 0.1 M NaCl solutions involving potentiodynamic polarization curves, electrochemical impedance spectroscopy (EIS) and scanning vibrating electrode (SVET) techniques. Furthermore, an analysis after 96 h of exposure to salt mist test simulating a corrosive attack in harsh environment is presented, too. The obtained results showed enhanced corrosion resistance of the ternary alloys electrodeposited under PC conditions (the best for 1.67 Hz frequency) as compared to those using DC. Additionally, Raman spectroscopy evidenced the presence of tin oxi/hydroxy chloride and tin oxides as surface corrosion products. A corrosion mechanism has been proposed.

  • 12.
    Uczak de Goes, Wellington
    et al.
    University West, Trollhättan, Sweden.
    Markocsan, Nicolaie
    University West, Trollhättan, Sweden.
    Gupta, Mohit
    University West, Trollhättan, Sweden.
    Vaßen, Robert
    Forschungszentrum Jülich, Germany.
    Matsushita, Taishi
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Illkova, Kseniya
    Institute of Plasma Physics, Prague, Czech Republic.
    Thermal barrier coatings with novel architectures for diesel engine applications2020Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 396, artikel-id 125950Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    The increased demands for higher efficiency and environmentally friendly diesel engines have led to a continuous search for new coating processing routes and new ceramic materials that can provide the required properties when applied on engine components such as pistons and exhaust manifolds. Although successful in gas turbine applications, thermal barrier coatings (TBCs) produced by suspension plasma spraying (SPS) processes have not been employed so far in the automotive industry. This work aims to achieve a better understanding of the role of thermal conductivity and thermal effusivity on the durability of SPS TBCs applied to pistons of diesel engines. Three different coating architectures were considered for this study. The first architecture was yttria-stabilized zirconia (YSZ) lamellar top coat deposited by APS (Atmospheric Plasma Spray) and used as a reference sample in this study. The second architecture was a columnar SPS top coat of either YSZ or gadolinium zirconate (GZO) while the third architecture was an SPS columnar top coat, “sealed” with a dense sealing layer deposited on the top coat. Two types of sealing layers were used, a metallic (M) or a ceramic thermal spray layer (C). Laser Flash Analysis (LFA) was used to determine the thermal conductivity and thermal effusivity of the coatings. Two different thermal cyclic tests were used to test the TBCs behavior under cyclic thermal loads. Microstructure analysis before and after the thermal cyclic tests were performed using SEM in different microstructures and materials. The thermal cyclic test results were correlated with coatings microstructure and thermophysical properties. It was observed that the columnar coatings produced by SPS had an enhanced service life in the thermal cyclic tests as compared to the APS coatings. 

  • 13. Valizadeh, S.
    et al.
    Holmbom, G.
    Leisner, Peter
    Högskolan i Jönköping, Tekniska Högskolan, JTH, Data- och elektroteknik.
    Electrodeposition of Cobalt-Silver Multilayers1998Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 105, nr 3, s. 213-217Artikel i tidskrift (Refereegranskat)
  • 14.
    Zhu, Baiwei
    et al.
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Zanella, Caterina
    Jönköping University, Tekniska Högskolan, JTH, Material och tillverkning.
    Influence of Fe-rich intermetallics and their segregation on anodising properties of Al-Si-Mg rheocast alloys2021Ingår i: Surface & Coatings Technology, ISSN 0257-8972, E-ISSN 1879-3347, Vol. 422, artikel-id 127570Artikel i tidskrift (Refereegranskat)
    Abstract [en]

    During rheocasting of Al alloys, the component's surface can be enriched in Fe-rich intermetallics due to the surface liquid segregation or the interaction with the die material. Although this precipitates enrichment affects only the surface, it can have a big impact on the quality of the surface treatments or durability. In this paper, the effect of Fe-rich intermetallics on the hardness and corrosion resistance of the anodized layer of AlSiMg alloys was examined by using nanoindentation and electrochemical impedance spectroscopy (EIS) techniques. A sulfuric acid anodising process was performed on unground and mechanical ground surfaces of TX630 substrates produced by the rheocasting process. During anodising, Fe-rich intermetallics can be dissolved, leaving voids in the oxide during its growth. The anodised samples with two different oxide layer thickness (4 and 7 μm) were tested by EIS in 3 wt-% NaCl solution for 12 h. A comparison of the EIS results of unground and mechanically ground surfaces demonstrated that the mechanical grinding successfully removed the Fe enriched layer, improving corrosion protection of the anodised oxide. Moreover, the hardness measurements indicate that the oxide layer on the mechanically ground surface with low Fe content shows higher hardness than on the unground surface with high Fe content.

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