This article presents results of experimental evaluation of glob-top materials for multi-chip-modules (MCM) in harsh environments. Material and process tests have been performed with the purpose to find a material which would fulfill the reliability requirements for use e.g. in military or automotive applications. Seven polymer materials, i.e. four epoxies, two silicones and one polyurethane material have been selected and evaluated in the experiments. The most critical material and process parameters for glob-top have been identified and measured. Based on the experimental results, application-based scoring of studied epoxy materials has been performed. Material evaluation results have been summarized in conclusions about the most suitable glob-top material for use in harsh environments.